ASTM D1552 PDF

ASTM-D – Download as PDF File .pdf), Text File .txt) or read online. Find the most up-to-date version of ASTM D at Engineering This application note demonstrates detemination of sulfur in hydrocarbon fuels by LECO CHN with Sulfur Add-On Module (S) in accordance with ASTM.

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Resistance—Type Furnace Assemble the apparatus according to the instructions furnished by the manufacturer. A framework, a supreme code of conduct cherishes us every day to serve the world better.

Iron-Chip Accelerator having a sulfur content of notmore than 0. Starch-Iodide Solution—Make a paste by adding 9 g of soluble starch to 15 mL of water.

Preparation of Apparatus Induction-Type Furnace Assemble the apparatus according wstm the instructions furnished by the manufacturer.

ASTM D – 03 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)

This service is not available if you are a URL user where you do not log in with an email address. It is the responsibility of the d155 of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Atsm, as described in Test Method D Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. A microprocessor calculates the aastm percent sulfur from the sample weight, the integrated detector signal and a predetermined calibration factor. To assure that the furnace is in proper adjustment and that its operation produces acceptably high temperature, potassium alum is employed for standardizing the apparatus.

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Sulfur content in Petroleum Products by ASTM D

The additional equipment required is dependent on the type of furnace used and is astn from the manufacturer of the specific combustion unit. For earlier information on the deleted procedures, D —08 may be perused. For IR detectiondetermine and load the microprocessor with the calibration factor for the particular type of sample to be analyzed lubricating oil, petroleum coke, residual fuel as recommended by the manufacturer.

Work Item s – proposed revisions of this standard. Sampling Take f1552 in accordance with the instructions in Practice D Use the same materials in the determination of the alum and standardization factors as for the unknown samples. Quantity of the sample. Because effects such as sample volatility can also affect the relative recovery as SO2 of the sulfur originally present in the sample, it is necessary to determine a standardization factor.

You need to log in before adding standards to the monitoring service. Vanadium Pentoxide, anhydrous, powdered V2O5.

Each holder can be adjusted independently. The moment new editions of the standards you monitor are released, changes are made, or appendixes are published, you will be alerted by email.

Standards monitoring is a free service designed for you who wish to be alerted of changes to or new editions of the standards required in your work. Beret, standard mL or automatic types available from the manufacturers of the specific combustion units, are suitable. Insert a small glass-wool plug in the upper end of the glass tubing connecting the furnace with the absorber to catch oxides of tin.

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Tin 20 to mesh. The adjustment range should not less than 15 mm.

Calculate the standardization factor as follows: Potassium Iodate, Standard Solution 0. Two of the three procedures use iodate detection ; one employing an induction furnace for pyrolysis, the other a resistance furnace.

ASTM D1552 – 16E1

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Sulfur with the chemical symbol S is the chemical element that is in the sixth and third groups of the periodic table of elements. Since these procedures are no longer being used in the industry laboratories based on a survey of D In other cases the presence of sulfur compounds is detrimental to the processing or use of the product. Connect a rotameter between the purifying train and the furnace.

You need to log in before adding standards to the monitoring service. Start Webshop Product catalog Product presentation. Nitrogen when present in excess of 0. With the correct amount of iron chips, weighed to For example, V2O5 has a definite effect and should be included if wstm for unknowns as recommended in the procedure with the resistance-type furnace.